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High Pressure

A high pressure facility is now available for all magnets at NHMFL to perform both electrical transport and optical measurements over a wide range of sample volumes and attainable pressures under conditions of both hydrostatic and uniaxial stress. Conventional miniature piston-cylinder cells that can reach 1.7 GPa and have provisions for fiber optic access and electrical leads are available, but the main thrust in high pressure techniques is focused on diamond-anvil cell [DAC] technology. Although the available sample space in a DAC is small (typically a 300-700 um diameter cylinder, 60-120 um thick), two to six electrical leads can be attached to single crystal platelets only 100 um on an edge and as thick as 40 um. Spectroscopic measurements are limited only by the 10 kN load that the DAC can sustain and the optical window material, diamond. Type II diamond anvils will be available for infrared studies. UV studies can be carried out in a sapphire-ball cell designed by Professor Daniels from the University of Delaware.

To address the experimental restrictions of sample orientation and cryogenic temperatures in DC and pulsed magnetic fields, three different DACs have been designed (see table below). All are made entirely of BeCu and have optical ports and provisions for either miniature triaxial cable or shielded twisted pairs. The largest of the three DACs provides the highest pressures. DAC #2 was designed with its small diameter and thin wall to minimize eddy current heating of the sample prior to data acquisition in pulsed magnets. This particular cell is small enough to freely rotate within a 12 mm sphere and thus enables orientation dependent work to millikelvin temperatures and pulsed fields to 50 T and higher. Both cells #1 & #2 support a minimal load of 10 kN. DAC #3 is intended for microkelvin work and possibly heat capacity studies.

Characteristics of Pressure Cells Available at NHMFL
Pressure
Cell
Mass
(g)
Pressurized
Volume
(Dia.XHeight)
(mm X mm)
Radius Of
Sphere Of
Free Rotation
(mm)
Max Magnetic
Field To Date
(T)
Max
Pressure
To Date
GPa
DAC #1 22.3 0.6 X 0.09 20.3 mm 20 T DC 14.0
DAC #2 4.0 0.5 X 0.08 12.0 50 T pulsed, 98%
penetration
4.0
DAC #3 1.7 0.4 X 0.08 9.0 --- 2.2
DAC #4 1.1 0.3 X 0.06 7.0 --- ---
Piston-Cylinder 31 3.3 X 4.5 --- 20 T 1.7
Sapphire Ball 61 1.0 X 0.3 --- --- 7.8
Users planning high pressure experiments in the NHMFL facilities should answer some questions about their sample(s).

Photo Caption: Diamond anvil cells are available for optical and transport measurements in both pulsed and DC fields. The upper photo shows a disassembled DAC #1. DAC numbers 1, 2, and 3 are shown assembled in the lower picture.
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Curator: Scott Hannahs <sth@magnet.fsu.edu>
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